Structure

    redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-2H,0,redEnd

Rainbow trout gastrointestinal mucus, mucin production, mucin glycosylation and response to lipopolysaccharide

GlyTouCan Accession Number: Loading...

Peak Intensity
260.48 2.1
335.83 2.5
348.09 15.2

Annotations:

B b1D-Gal,p/#bcleavage--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd
384.0 3.1

Annotations:

YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6b1D-GlcNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
437.39 1.5

Annotations:

^{2,4}X_{GlcNAc} redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6b1D-GlcNAc,p/#xcleavage_2_4$MONO,Und,-2H,0,redEnd
447.01 5.2

Annotations:

YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p/#ycleavage$MONO,Und,-2H,0,redEnd
447.35 3.0
447.75 7.1
470.52 1.5
475.03 1.3
478.49 3.4
510.13 1.5

Annotations:

B ?1D-GalNAc,p/#bcleavage--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd B b1D-GlcNAc,p/#bcleavage--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd
515.77 8.4
516.35 2.2
528.27 2.3

Annotations:

C ?1D-GalNAc,p/#ccleavage--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd C b1D-GlcNAc,p/#ccleavage--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd
542.43 1.9
547.87 1.5
566.98 2.1
576.36 1.6
584.76 8.7
590.38 2.9
608.34 2.5
613.66 1.3
619.11 2.6
622.02 68.5

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-2H,0,redEnd Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p/#ycleavage$MONO,Und,-2H,0,redEnd
622.34 28.9
623.42 1.5
625.31 1.7
631.49 5.7
632.3 2.6

Annotations:

ZZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6b1D-GlcNAc,p(--3a1L-Fuc,p/#zcleavage)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#zcleavage$MONO,Und,-2H,0,redEnd ZZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#zcleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#zcleavage$MONO,Und,-2H,0,redEnd ZZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#zcleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p/#zcleavage)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-2H,0,redEnd
643.05 1.7
665.85 1.3
669.31 8.2
675.71 3.0
676.3 2.9
681.4 2.6
684.46 1.4
689.46 2.4
690.28 7.6
690.49 3.0
690.93 8.5
694.37 1.6
698.22 7.5
702.95 4.3
708.41 1.9
713.74 2.2

Annotations:

CZ ?1D-GalNAc,p/#ccleavage--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#zcleavage$MONO,Und,-H,0,redEnd BY ?1D-GalNAc,p/#bcleavage--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#ycleavage$MONO,Und,-H,0,redEnd BY ?1D-GalNAc,p/#bcleavage--6b1D-GlcNAc,p(--3a1L-Fuc,p/#ycleavage)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd CZ ?1D-GalNAc,p/#ccleavage--6b1D-GlcNAc,p(--3a1L-Fuc,p/#zcleavage)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd
714.45 7.6

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#zcleavage$MONO,Und,-2H,0,redEnd Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6b1D-GlcNAc,p(--3a1L-Fuc,p/#zcleavage)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-2H,0,redEnd Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#zcleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-2H,0,redEnd
714.99 1.9
715.46 8.1

Annotations:

YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#zcleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#ycleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p/#zcleavage$MONO,Und,-H,0,redEnd Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6b1D-GlcNAc,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
730.07 3.4
730.95 2.1

Annotations:

CY ?1D-GalNAc,p/#ccleavage--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#ycleavage$MONO,Und,-H,0,redEnd CY ?1D-GalNAc,p/#ccleavage--6b1D-GlcNAc,p(--3a1L-Fuc,p/#ycleavage)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd
731.17 1.3
733.07 3.5
733.29 8.1

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6b1D-GlcNAc,p/#ycleavage$MONO,Und,-H,0,redEnd YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#ycleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
734.26 10.5
738.21 2.0
741.36 3.4
751.66 1.4
752.08 1.8
753.59 1.3
754.16 3.5
755.96 4.3
756.73 2.9
757.82 1.9
766.8 8.1
768.81 1.7
773.86 1.7
828.46 1.6
835.07 2.2
859.63 2.4

Annotations:

ZZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#zcleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p/#zcleavage$MONO,Und,-H,0,redEnd B ?1D-GalNAc,p/#bcleavage--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd
877.71 2.6

Annotations:

YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p/#zcleavage$MONO,Und,-H,0,redEnd C ?1D-GalNAc,p/#ccleavage--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#zcleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
878.38 3.0
882.37 2.7
895.29 19.8

Annotations:

YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
895.6 9.9

Annotations:

YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
896.68 4.6
900.43 11.1

Annotations:

ZZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#zcleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd ZZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#zcleavage$MONO,Und,-H,0,redEnd ZZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6b1D-GlcNAc,p(--3a1L-Fuc,p/#zcleavage)--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd ZZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p/#zcleavage)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd
1014.45 2.3
1032.23 9.9
1032.51 2.3
1033.63 4.3
1063.67 2.6
1064.26 4.9

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd
1064.55 3.6
1065.44 3.6
1080.17 4.0

Annotations:

YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#ycleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p/#zcleavage$MONO,Und,-H,0,redEnd YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#zcleavage$MONO,Und,-H,0,redEnd YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6b1D-GlcNAc,p(--3a1L-Fuc,p/#ycleavage)--4b1D-Gal,p--??1D-GalNAc,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6b1D-GlcNAc,p(--3a1L-Fuc,p/#zcleavage)--4b1D-Gal,p--??1D-GalNAc,p/#ycleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#zcleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p/#ycleavage$MONO,Und,-H,0,redEnd YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p/#zcleavage)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#zcleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#ycleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#zcleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p/#ycleavage)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd
1080.54 1.9
1081.42 1.7
1082.07 1.3

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#ycleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd
1104.76 1.7
1184.47 2.5
1185.25 1.9
1187.49 2.3
1202.8 2.1
1226.77 2.7

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#zcleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p/#zcleavage$MONO,Und,-H,0,redEnd
1227.25 2.0
1229.67 2.3
1244.69 69.2

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6b1D-GlcNAc,p(--3a1L-Fuc,p)--4b1D-Gal,p--??1D-GalNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
1245.58 25.6
1566.81 2.5

There are not related spectra

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 1592.62
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

N/A

HPLC

Column

Method

  • 40 min gradient with 10 ul/min run rate
  • 10 mM (NH4)HCO3 in water
  • 10 mM (NH4)HCO3 in 80% acetontirile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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