Structure

    redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-2H,0,redEnd

Rainbow trout gastrointestinal mucus, mucin production, mucin glycosylation and response to lipopolysaccharide

GlyTouCan Accession Number: Loading...

Peak Intensity
204.05 4.6

Annotations:

YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#ycleavage)--6a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
272.03 5.6

Annotations:

BZ ?1D-GalNAc,p/#bcleavage--6a2D-NeuAc,p--8a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd
276.27 4.4
290.17 113.5

Annotations:

B a2D-NeuAc,p/#bcleavage--8a2D-NeuAc,p$MONO,Und,-H,0,redEnd
291.03 17.0
291.32 5.7
299.2 6.5

Annotations:

C ?1D-GalNAc,p/#ccleavage--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-2H,0,redEnd
299.67 3.5
302.43 6.2
348.28 3.9

Annotations:

B b1D-Gal,p/#bcleavage--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd ZZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#zcleavage)--6a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd
384.22 15.2

Annotations:

YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
384.49 6.6
385.16 5.1
407.15 3.2
408.11 4.6
433.05 4.1
452.62 7.8
453.4 3.9
468.34 4.3
469.25 7.1
473.8 8.2

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#zcleavage)--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-2H,0,redEnd
483.16 15.8

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-2H,0,redEnd
483.95 5.5
484.91 3.9
489.77 3.2
493.4 4.3
504.3 4.1
511.27 11.9

Annotations:

^{0,2}A_{NeuAc} a2D-NeuAc,p/#acleavage_0_2--8a2D-NeuAc,p$MONO,Und,-H,0,redEnd Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6a2D-NeuAc,p--8a2D-NeuAc,p/#ycleavage$MONO,Und,-2H,0,redEnd
521.19 13.1
524.35 6.2
533.42 5.9
537.78 5.7
538.05 5.1
538.35 7.5
546.87 20.2
547.85 6.1
548.54 5.5
551.29 9.6

Annotations:

ZZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#zcleavage)--6a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd
552.3 3.6
554.29 4.2
556.9 3.6
563.13 3.5
566.23 4.0
568.18 3.2
568.89 3.2
569.35 4.0

Annotations:

YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#ycleavage)--6a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#zcleavage)--6a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
575.95 9.0
576.4 3.4
577.54 6.6
580.78 9.6
581.38 55.7

Annotations:

B ?1D-GalNAc,p/#bcleavage--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-H,0,redEnd
581.76 9.4
582.36 17.8
583.27 3.5
586.04 10.0
587.86 4.8
588.8 8.8
593.4 5.1
594.4 3.2
595.28 14.7
597.11 5.2
598.88 6.2
599.36 8.0

Annotations:

C ?1D-GalNAc,p/#ccleavage--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-H,0,redEnd
600.93 3.2
610.12 4.0
613.24 12.5
614.18 3.3
617.22 7.3
617.96 3.6
621.59 5.7
622.2 8.8
626.86 4.8
627.69 13.9
627.94 11.4
628.16 4.5
658.18 4.4
675.5 4.1

Annotations:

YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6a2D-NeuAc,p--8a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
678.16 3.6
733.41 17.5

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
743.63 3.6
768.09 4.7
786.67 3.2

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-H,0,redEnd
787.49 6.9
878.21 3.7

Annotations:

YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#ycleavage)--6a2D-NeuAc,p--8a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
906.34 3.6
928.23 3.5
930.31 21.9
930.62 8.2
946.56 3.8
948.02 6.2
948.56 16.6

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p/#zcleavage)--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-H,0,redEnd
949.62 16.2
1006.44 34.2

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6a2D-NeuAc,p--8a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd
1007.74 4.3
1024.59 175.9

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6a2D-NeuAc,p--8a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
1025.65 74.6
1026.59 20.6
1073.51 4.7
1134.76 4.8
1135.92 5.2

There are not related spectra

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 1314.49
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

N/A

HPLC

Column

Method

  • 40 min gradient with 10 ul/min run rate
  • 10 mM (NH4)HCO3 in water
  • 10 mM (NH4)HCO3 in 80% acetontirile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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